Tag: Thermal Analysis

DSC 600

DSC 600 Differential Scanning Calorimeter ● Flexible cooling systems: water, mechanical, or liquid nitrogen (LN2). ● Ultra-light mineral furnace design reduces heat loss and enhances thermal uniformity. ● Optional high-pressure DSC model supports measurements up to 1000 psi.

AMI Instruments
DSC 600

Differential Scanning Calorimeter

  • Flexible cooling systems: water, mechanical, or liquid nitrogen (LN2)
  • Ultra-light mineral furnace design reduces heat loss and enhances thermal uniformity
  • Optional high-pressure DSC model supports measurements up to 1000 psi

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DSC 600 Differential Scanning Calorimeter ● Flexible cooling systems: water, mechanical, or liquid nitrogen (LN2). ● Ultra-light mineral furnace design reduces heat loss and enhances thermal uniformity. ● Optional high-pressure DSC model supports measurements up to 1000 psi.

The DSC 600 from Advanced Measurement Instruments (AMI) is the next generation of Differential Scanning Calorimeters (DSC), crafted to meet the evolving needs of professionals in materials research, chemical engineering, quality control, petrochemicals, and pharmaceuticals. Designed for precision, reliability, and affordability, the DSC 600 sets new standards in thermal analysis.

At the heart of the DSC 600 is its innovative heat flux plate, engineered to capture the smallest energy changes with unmatched sensitivity and accuracy. This powerful capability enables precise measurements across a broad spectrum of applications, including enthalpy, glass transition, heat of crystallization, purity determination, and heat capacity.

Equipped with an ultra-light furnace, the DSC 600 ensures excellent thermal conductivity and stability, delivering consistent performance across a wide temperature range. With a selection of specialized heat flux plates, it can be tailored to meet diverse testing needs,enhancing efficiency and flexibility in every lab.

  • Key Features

    Precision

    High-sensitivity heat flow sensor platform delivers calorimetric accuracy of ±0.1%. With four distinct heat flow sensor types available, it comprehensively meets the precise measurement needs of diverse materials, accommodating a wide range of experimental and application scenarios.

    Featuring innovative furnace technology and unique sensor design, the system achieves exceptional baseline repeatability while offering low noise, high sensitivity, and outstanding resolution. This ensures the detection of even minute thermal changes that might otherwise be lost in noise.

    Stability

    The mineral-insulated furnace body design combines excellent thermal conductivity with corrosion resistance, while dual-PID temperature control ensures data accuracy and stability.

    Advanced circumferential heating technology and a proprietary dual-PID control system guarantee precise adherence to programmed temperature profiles during both heating and cooling phases. With temperature control accuracy of ±0.01°C, the system significantly minimizes thermal fluctuations that could compromise experimental results.

    Ease of Use

    The intuitive software interface features streamlined UI and modular architecture, enabling effortless operation. Researchers can quickly master experimental setup, data analysis, and all critical workflows.

    The maintenance optimized furnace design allows easy cleaning even after sample contamination during loading, significantly enhancing experimental efficiency while extending equipment service life.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    High-Precision Heat Flow Sensor

    The self-developed high-sensitivity heat flow sensor platform delivers low noise, high sensitivity, and exceptional resolution to reliably detect minute thermal variations that might otherwise be obscured by noise.

    Four Types of Heat Flow Sensors

    The DSC600 offers four types of heat flow sensor platforms: standard testing type, high-sensitivity type (for biopharmaceutical materials), corrosion-resistant type (for corrosive samples), and energetic materials type (for chemical reactions). These sensors meet the requirements of different application scenarios and sample types.

    Precision Temperature Control

    The system utilizes circumferential heating technology and a proprietary dual-PID control system to ensure exact adherence to programmed temperature curves during heating/cooling processes. With a temperature control accuracy of ±0.01°C, it effectively minimizes thermal fluctuations that could compromise experimental results.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Ultralight Mineral Furnace

    The silver-constructed furnace body delivers exceptional thermal conductivity and stability, ensuring precise temperature control and rapid thermal response. The pure silver material effectively minimizes heat loss while enhancing analytical efficiency, achieving uniform heating/cooling across samples. Its superior corrosion resistance extends instrument service life, accommodating diverse experimental environments.

    Automatic Gas Switching Control

    The multi-channel gas inlet device enables automatic gas switching during experiments. This integrated unit combines four or six gas lines into a single module to meet the demands of frequent gas changes across different testing procedures.

    Gas Preheating Function

    The furnace incorporates heated gas lines at the inlet ports, enabling gas preheating before entering the sample chamber. This design stabilizes experimental conditions and enhances testing efficiency.

    Three High-Efficiency Cooling Systems

    The DSC 600 is equipped with three high-efficiency cooling systems, offering versatile refrigeration options: water bath cooling, mechanical refrigeration, and liquid nitrogen cooling.

    The water bath cooling system regulates furnace temperatures from 10°C to 600°C, ideal for scenarios not requiring cryogenic conditions, such as polymer melting point and crystallization temperature analysis. The mechanical refrigeration system covers a temperature range of -90°C to 450°C, widely used in polymer material analysis, including glass transition studies, crystallization kinetics research, and conventional low-temperature testing applications.

    The liquid nitrogen cooling system utilizes the endothermic properties of evaporating liquid nitrogen for rapid cooling, with a furnace temperature range of -150°C to 600°C. It is primarily employed for ultra-low temperature research, such as metal alloy phase transitions, superconducting material analysis, and rapid quenching experiments, including amorphous material preparation and fast cooling process studies.

  • Software

    Standard Functions:

    ✔️ Glass transition analysis (2-point or 6-point method)

    ✔️ Onset/peak temperature determination

    ✔️ Peak integration

    ✔️ Melting peak analysis

    ✔️ Crystallinity measurement

    ✔️ Data smoothing

    ✔️ Baseline correction

    Optional Functions:

    Specific Heat Capacity: The system rapidly determines specific heat values by testing samples alongside reference materials with known heat capacity (e.g., sapphire) under identical conditions.

    AMI Instruments DSC 600
Differential Scanning Calorimeter
    Experiment Program Setup Interface
  • Applications

    Cold Crystallization Behavior of PET

    The crystal growth and degree of crystallization depend on the polymer type, cooling rate, or isothermal aging time. The calculation method for crystallization enthalpy is the same as that for melting enthalpy. Cold crystallization is the process of crystal growth during heating. This exothermic event precedes crystal melting.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Glass Transition Analysis

    The glass transition temperature (Tg) of polymers refers to the temperature range at which they transition from a rigid “glassy” state to a flexible “rubbery” state, significantly affecting their usability, particularly in elastomers. Understanding Tg is crucial for quality control, process optimization, ensuring product performance, and maintaining material consistency.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Phase Transformation of Nickel-Titanium Alloys

    The Af temperature refers to the phase transition temperature of nickel-titanium alloys, marking the transformation from the high-temperature phase (a-phase) to the low-temperature phase (f-phase). In the high-temperature phase, the crystal structure of nickel-titanium alloy exhibits a cubic system, while in the lowtemperature phase it transforms into a monoclinic system. This phase transition temperature change gives nickel-titanium alloys their shape memory properties. These shape memory characteristics enable important applications across various fields, such as medical devices, aerospace, and mechanical engineering.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Typical Applications

    ✔️ Melting Temperature

    ✔️ Crystallization Temperature

    ✔️ Heat of Chemical Reaction

    ✔️ Glass Transition Temperature

    ✔️ Specific Heat Capacity

    ✔️ Degree of Crystallinity

    ✔️ Degree of Cure

    ✔️ Oxidative Stability

    ✔️ Thermal Stability

    ✔️ Solid-State Phase Transition

    ✔️ Liquid Crystal Phase Transition

    ✔️ Aging of Materials

    ✔️ Polymorph

    Materials

    ✔️ Thermoplastics
    ✔️ Thermosets
    ✔️ Rubbers
    ✔️ Catalysts
    ✔️ Phenolics
    ✔️ Pharmaceuticals
    ✔️ Chemicals
    ✔️ Coals and other fuels
    ✔️ Nuclear Research
    ✔️ Foods
    ✔️ Cosmetics
    ✔️ Explosives

  • Specifications

    Specification Option 1 Option 2 Option 3
    Temperature Range -150~600°C
    Temperature Accuracy ±0.1°C
    Temperature Precision ±0.01°C
    Program Rate 0.1~200°C/min
    Cooling Mode Water Cooling Refrigerated Cooling Liquid Nitrogen Cooling
    Maximum Temperature 600°C 450°C 600°C
    Minimum Temperature Ambient Temperature -40°C or -90°C -150°C
    Calorimetric Accuracy ±0.1%
    Noise 0.5 μW
    Gas Nitrogen, Argon, Helium, Compressed Air, Oxygen, etc.
    Sampling Frequency 10 Hz
    Weight 27 lbs.
    Dimensions 17 in (W) × 17 in (D) × 9.5 in (H)
    Options
    Gas Controller 4 Channel Automatic Gas Switching
    Software Functions Specific Heat Capacity
  • Accessories

    Crucibles

    Crucibles serve as sample containers in thermal analysis measurements, effectively protecting sensors and preventing measurement contamination. The selection of crucible type is critical for result quality. We offer various crucible options to meet different testing requirements, ensuring accurate and reliable measurement results.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Pellet Press

    The crucible pellet press elevates sample encapsulation to higher performance and convenience, suitable for routine and hermetic testing of various materials. The standard model is specifically designed for solid sample crucibles, while the universal model handles both solid and liquid sample crucibles, offering greater flexibility for your experiments.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Fully Automated Chiller

    The fully automated recirculating bath enables precise continuous temperature control within the range of -10°C to 90°C. When coupled with the water-cooled DSC 600 system, it achieves rapid furnace cooling, significantly enhancing experimental efficiency.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

    Gas Selector Accessory

    The gas selector supports one-button switching across multiple gases, accommodating up to 4 input ports. It simplifies valve disassembly and assembly when sampling different gases, effectively minimizing leakage risks associated with manual handling. Additionally, the instrument features an automatic purging process, ensuring efficient gas line purification and seamless, automated switching between gases.

    AMI Instruments DSC 600
Differential Scanning Calorimeter

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STA 650/1200/1500

STA 650/1200/1500 Simultaneous Thermal Analyzer ● Simultaneous measurement of TGA and DSC (DTA) for comprehensive thermal analysis. ● Optimized for evolved gas analysis with high-resolution detection of micro-scale mass. ● Micro furnace design significantly reduces gas buoyancy and enhances baseline stability.

AMI Instruments
STA 650/1200/1500

Simultaneous Thermal Analyser

  • Simultaneous measurement of TGA and DSC (DTA) for comprehensive thermal analysis.
  • Optimized for evolved gas analysis with high-resolution detection of micro-scale mass
  • Micro furnace design significantly reduces gas buoyancy and enhances baseline stability

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brochure
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quote

STA 650/1200/1500 Simultaneous Thermal Analyzer ● Simultaneous measurement of TGA and DSC (DTA) for comprehensive thermal analysis. ● Optimized for evolved gas analysis with high-resolution detection of micro-scale mass. ● Micro furnace design significantly reduces gas buoyancy and enhances baseline stability.

AMI is pleased to introduce the next-generation STA (Simultaneous Thermal Analyzer), a state-of-the-art instrument for advanced thermal analysis.
Incorporating a 0.1-microgram balance resolution, sophisticated control algorithms, and an innovative hang-down design, the STA offers exceptional precision and reliability in a cost-effective, high-performance system.

The STA Series enables simultaneous Thermogravimetric Analysis (TGA) and Differential Scanning Calorimetry (DSC) or Differential Thermal Analysis (DTA) on a single sample within a single test cycle. Built for precision and reliability, the STA delivers comprehensive thermal profiles without the need for running multiple experiments, ultimately saving you both time and valuable sample material.

Engineered for quality control, routine testing, academic research, and industrial R&D, the STA Series combines robust construction with user-friendly software for a cost-effective solution in high-precision thermal analysis.

The STA is powered by Infinity Pro Thermal Analysis software, a simple Windows-based platform that provides all the essential features needed to analyze and interpret your thermal data.

  • Key Features

    True Hang-Down Balance Design

    Industry-leading stability, sensitivity, and long-term drift resistance for reliable and repeatable measurements without the need for buoyancy corrective experiments.

    High Sensitivity Microbalance

    Sub-microgram-level accuracy across a broad temperature range, providing confidence in your thermal and mass loss data.

    24-Bit Resolution

    High-precision measurement of temperature, delta T, and weight with minimal noise and high digital fidelity.

    Small Swept Volume Furnace Cup (7.5mL)

    Enhances temperature uniformity and gas exchange efficiency.

    Simultaneous TGA/DSC or DTA

    Perform thermogravimetric and calorimetric analyses in a single run— ideal for decomposition, oxidation, and phase transitions.

    Dual Purge Gas System

    Separate channels for purge and protective gases allow for fine control of the experimental atmosphere.

    Broad Temperature Range

    Furnace operation up to 1500°C under inert, oxidizing, or reducing gas environments.

    Motor-Driven Furnace Lift

    Ensures automated, smooth movement of the furnace for consistent sample positioning.

  • Specifications

    Specification -40°C – 650°C Ambient – 1200°C Ambient – 1500°C
    Temperature -40°C – 650°C Ambient – 1200°C Ambient – 1500°C
    Programmed Rate 0.1 – 100 °C/min 0.1 – 40 °C/min
    DSC Sensitivity < 1 μW < 4 μW
    TGA Measuring Range +/- 200 mg
    TGA Readability 0.1 μg
    Thermocouple Type K Type R
    DSC / DTA Mode Yes
  • Capabilities

    Evolved Gas Analysis (EGA) Compatibility

    Interface with mass spectrometry (MS) or FTIR systems for evolved gas studies during thermal decomposition.

    4-Gas Selector System

    Automates delivery of up to four different gases for programmable switching during analysis.

    Sub-Ambient System (650°C Model)

    Low-temperature furnace models support experiments starting below room temperature

    High-Temperature Flexibility

    Optional DSC-only high-temperature mode to allow DSC-only to 1,500°C
    Optional TGA-only high-capacity mode for larger or reactive samples

    For more details about the additional customization options or to request a quote, Explore additional options for your STA Instrument.

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TGA 1000/1200/1500

TGA 1000/1200/1500 Thermogravimetric Analyzer ● Temperature range options: ambient to 1000°C / 1200°C / 1500°C. ● Insulated balance housing minimizes thermal drift and ensures accurate mass measurements. ● Combines high sensitivity, low drift design, and robust thermal insulation.

AMI Instruments
TGA 1000/1200/1500

Thermogravimetric Analyser

  • Temperature range options: ambient to 1000°C / 1200°C / 1500°C.
  • Insulated balance housing minimizes thermal drift and ensures accurate mass measurements.
  • Combines high sensitivity, low drift design, and robust thermal insulation.
  • Download
    brochure
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    quote

    TGA 1000/1200/1500 Thermogravimetric Analyzer ● Temperature range options: ambient to 1000°C / 1200°C / 1500°C. ● Insulated balance housing minimizes thermal drift and ensures accurate mass measurements. ● Combines high sensitivity, low drift design, and robust thermal insulation.

    The TGA Series combines research-grade capabilities with an accessible price point, delivering high-performance thermal analysis tools without compromising on quality. Equipped with advanced high-sensitivity microbalances and compact, state-of-the-art furnaces, these instruments provide unparalleled precision, drastically reduce buoyancy effects, and ensure superior temperature responsiveness.

    Renowned for their reliability and versatility, the TGA Series instruments are trusted across a wide range of industries, including plastics, rubber, adhesives, fibers, pharmaceuticals,environmental energy, petrochemicals, and food science. These instruments meet critical customer needs by enabling the characterisation and analysis of parameters such as material decomposition temperatures, mass loss percentages, component contents, and residual mass.

    • Key Features

      Proprietary Microbalance

      The proprietary TGA microbalance combines high sensitivity, low drift technology, and thermal insulation design to deliver exceptional weighing accuracy. With a resolution as precise as 0.1 μg, it is ideal for high-precision measurements of trace samples. The low-drift technology minimizes the impact of environmental factors, ensuring stable data even in long-duration experiments, while reducing errors caused by drift. Additionally, the thermal insulation design protects the balance from external temperature fluctuations, maintaining internal temperature stability and ensuring reliable results, even in conditions of rapid temperature change or high heat.

      Miniature Furnace

      The compact heating furnace is designed to significantly minimize gas buoyancy effects, ensuring that dynamic curve drift in TGA remains under 25 μg without requiring additional blank tests. Additionally, the furnace delivers a rapid temperature response, achieving heating rates of up to 300°C/min, which dramatically shortens experimental time and enhances overall work efficiency.

      Precise Temperature Control

      The advanced heating technology combined with a dual PID control system ensures precise adherence to the set temperature curve during both heating and cooling processes. With a temperature control accuracy of ±0.1°C, this system significantly reduces the influence of temperature fluctuations, delivering highly reliable experimental results.

      Multiple furnace options are available to meet the specific temperature
      requirements of different materials. With a maximum temperature
      capability of up to 1500°C, these furnaces are designed to satisfy the
      rigorous demands of both experimental and industrial applications.

      Wide Temperature Range

      Multiple furnace options are available to meet the specific temperature requirements of different materials. With a maximum temperature capability of up to 1500°C, these furnaces are designed to satisfy the rigorous demands of both experimental and industrial applications.

      Furnace Auto-Lift System

      The instrument is equipped with an automatic furnace lifting system, simplifying experimental operations and preventing equipment damage or safety incidents caused by improper manual handling.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Water Cooling System

      The fully automated recirculating bath provides precise and continuous temperature control, which effectively and rapidly reduces the TGA furnace temperature, significantly shortening the experimental time.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Automatic Gas Switching Control

      The gas selector supports one-button switching across multiple gases, accommodating up to 4 input ports. The device features an integrated design, consolidating four gas channels into a single module to meet the need for frequent gas switching during different testing processes.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Evolved Gas Analysis

      TGA can be combined with other analytical instruments for online monitoring and qualitative analysis of evolved gases, such as mass spectrometers (MS) or Fourier-transform infrared spectrometers (FTIR).

    • Software

      Standard Functions

      · 2-point or 6-point mass loss analysis

      · Peak temperature analysis

      · Weight loss step analysis

      · Mass loss initiation point

      · Residual mass calculation

      · 1st and 2nd derivative analysis

      · Data smoothing

      ·Baseline subtraction

      Optional Functions

      High-Resolution thermogravimetric analysis:
      Enables effective separation of overlapping mass loss regions, improving resolution, and quickly obtaining experimental data over a wide tempera-ture range.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer
      Experiment Program Setup Interface
    • Applications

      Materials

      – Petrochemical products
      – Coal and other fuels
      – Explosives
      – Cosmetics
      – Thermoplastic materials
      – Thermosetting materials
      – Rubber
      – Coatings
      – Elastomers
      – Polymers
      – Pharmaceuticals
      – Food Products
      – Catalysts
      – Chemicals
      – Asphalt
      – Ceramics

      Typical Applications

      – Thermal Stability
      – Thermal Pyrolysis
      – Oxidation Reactions
      – Dehydration Process
      – Decomposition
      – Process Kinetics
      – Combustion Process
      – Moisture Content
      – Residue and Ash Content

      Dynamic Baseline Drift

      In a typical TGA test, the sample mass may increase due to the “buoyancy effect” of the gas. However, the design of the miniature heating furnace ensures that the drift of the dynamic thermogravimetric curve remains below 25 μg, eliminating the need for baseline curve subtraction.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Weight Loss Step Analysis

      The analysis software enables clear observation of the weight loss ratio and corresponding temperatures at each stage of the process. For instance, the thermogravimetric curve of hydrated calcium oxalate demonstrates three distinct stages. In the first stage, bound water evaporates, producing water vapor and leaving behind calcium oxalate. In the second stage, calcium oxalate decomposes into calcium carbonate and carbon monoxide. Finally, in the third stage, calcium carbonate further breaks down into calcium oxide and carbon dioxide.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      High-Resolution TGA

      The high-resolution TGA technology intelligently adjusts the heating rate in response to the sample’s decomposition rate,effectively separating overlapping mass loss regions and enhancing resolution. This enables the rapid collection of experimental data across a wide temperature range. The exceptional resolution achieved with this advanced technology is particularly beneficial for analyzing the mass loss curve in TGA and the first derivative signals (DTG), providing highly detailed and accurate results.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer
    • Specifications

      Specification RT-1000°C RT-1200°C RT-1500°C
      Temperature Range RT-1000°C RT-1200°C RT-1500°C
      Temperature Accuracy ±0.5°C
      Temperature Precision ±0.1°C
      Program Rate 0.1-300°C/min 0.1-60°C/min
      Cooling Mode Water Cooling
      Resolution 0.1 μg
      Measuring Range ±200 mg
      Dynamic Baseline Drift ≤ 25 μg (No blank background subtraction)
      Isothermal Baseline Drift ≤ 5 μg/h
      Repeatability ≤ 10 μg
      Weight 44 lbs. (20 kg)
      Dimensions 16.3 in(W) × 14 in(D) × 16.6 in(H)
      Options
      Gas Controller 4-Channel Automatic Gas Switching
      Evolved Gas Analysis MS, FTIR, etc.
    • Accessories

      Crucibles

      Crucibles serve as sample containers in thermal analysis measurements, effectively protecting sensors and preventing measurement contamination. The selection of crucible type is critical for result quality. We offer various crucible options to meet different testing requirements, ensuring accurate and reliable measurement results.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Pellet Press

      The crucible pellet press elevates sample encapsulation to higher performance and convenience, suitable for routine and hermetic testing of various materials. The standard model is specifically designed for solid sample crucibles, while the universal model handles both solid and liquid sample crucibles, offering greater flexibility for your experiments.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Fully Automated Chiller

      The fully automated recirculating bath enables precise continuous temperature control within the range of -10°C to 90°C. When coupled with the water-cooled DSC 600 system, it achieves rapid furnace cooling, significantly enhancing experimental efficiency.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

      Gas Selector Accessory

      The gas selector supports one-button switching across multiple gases, accommodating up to 4 input ports. It simplifies valve disassembly and assembly when sampling different gases, effectively minimizing leakage risks associated with manual handling. Additionally, the instrument features an automatic purging process, ensuring efficient gas line purification and seamless, automated switching between gases.

      AMI Instruments TGA 1000/1200/1500
Thermogravimetric Analyzer

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