Tag: Surface Area

Meso 400

Gas Adsorption Meso 400 ● Balances high-throughput testing with independent station control. ● Available with 4 analysis ports, each with in-situ degassing capability. ● Simultaneously analyse different adsorbate gases across up to 4 stations.

AMI
Meso 400

Gas Adsorption Analyser 

  • Balances high-throughput testing with independent station control.
  • Available with 4 analysis ports, each with in-situ degassing capability.
  • Simultaneously analyse different adsorbate gases across up to 4 stations.

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quote

Gas Adsorption Meso 400 ● Balances high-throughput testing with independent station control. ● Available with 4 analysis ports, each with in-situ degassing capability. ● Simultaneously analyse different adsorbate gases across up to 4 stations.

The AMI-Meso 400 is a compact, high-performance sorption analyser designed for the precise characterisation of mesoporous and macroporous materials. Equipped with four fully independent analysis stations, it enables the determination of BET surface area, total pore volume, and pore size distribution with maximum efficiency.

Each analysis station features an individual dosing volume, allowing fully autonomous operation with independent programming and initiation at any time—eliminating downtime between analyses. This design ensures highly reproducible results and optimised throughput.

The AMI-Meso 400 supports a wide range of non-corrosive adsorptive gases, including N2, CO2, Ar, Kr, H2, O2, CO, NH₃, and CH4, providing exceptional flexibility for various research and industrial applications. Additionally, all four stations function as in-situ degassing units, enabling efficient sample preparation within the same system.

  • Key Features

    Module Design for Minimal Dead Volume

    The internal gas path design of the instrument adopts a unique integrated metal module design, which not only reduces the internal dead volume space but also helps mitigate possible leaks.

    Saturated Vapor Pressure P0

    An independent P0 pressure transducer is configured at 133 kPa for P0 value testing, enabling real-time P/P0 measurement for more accurate and reliable test data. Alternatively, an atmospheric pressure input method can be used to determine P0.

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    Independent analysis ports

    With independent analysis ports, the system employs a unique vacuum control logic that allows each station to operate without disruption, even when using a single mechanical pump or pump group. This enables simultaneous, independent experiments, meeting diverse adsorbent testing needs while ensuring high efficiency.

    Thermal Stabilisation

    A core rod in the sample tube reduces dead volume and stabilises the cold free space coefficient, while an iso-thermal jacket maintains a constant thermal profile along the tube. Additionally, automatic helium correction ensures precise calibration for any powder or particulate material, minimizing temperature-related deviations during analysis.

    High Accuracy Pressure Transducers

    Equipped with 1000 torr pressure transducers, the Meso Series enables precise physical adsorption analysis, achieving a partial pressure (P/P0) as low as 10-2 for nitrogen (N2) at 77 K.

    Optimised Manifold Contamination Control

    This system features a multi-channel, adjustable, and parallel vacuum design with segmented vacuum control. This setup effectively prevents samples from being drawn up into the analyser therefore preventing manifold contamination.

    Liquid Nitrogen Dewar

    The use of 1 L Dewar flasks in conjunction with a sealed cover ensures a stable thermal profile along the entire length of both the sample tubes and P0 tubes throughout the testing process.

    Sample Preparation

    Equipped with four in-situ degassing ports, enabling simultaneous degassing and analysis. Each port offers independent temperature control from ambient to 400°C, ensuring precise sample preparation.

  • Software

    PAS Software is an intelligent solution for operation control, data acquisition, calculation, analysis, and report generation on the Windows platform. It communicates with the host via the LAN port and can remotely control multiple instruments simultaneously.

    PAS Software adopts a unique intake control method, optimising pressure in the adsorption and desorption processes through a six-stage setting, which improves testing efficiency.

    Changes in pressure and temperature inside the manifold can be directly observed in the test interface, providing convenience for sample testing and instrument maintenance. The current state of analyser can be intuitively understood with the indicator light and event bar.

    Each adsorption equilibrium process is dynamically displayed on the test interface. Adsorption characteristics of the sample can be easily understood.

    A clear and concise report setting interface, including the following:

    Adsorption and desorption isotherms

    Single-/Multipoint BET surface area

    Langmuir surface area

    STSA-surface area

    Pore size distribution according to BJH

    T-plot

    Dubinin-Radushkevich

    Horvath-Kawazoe

    Saito-Foley

  • Applications

    Carbon Black

  • Technical Specs

    Model

    AMI Meso 400

    Analysis Ports

    4

    P0 Transducer

    4

    Analysis Pressure Transducer

    4

    Accuracy (Pressure Transducers)

    1000 Torr

    Pump

    1 mechanical pump (ultimate vacuum 10⁻² Pa)

    P/P0

    10⁻⁴ – 0.998

    Surface Area

    ≥ 0.0005 m²/g, test repeatability: RSD ≤ 1.0%

    Pore Size

    0.35–500 nm, test repeatability: ≤ 0.02 nm

    Pore Volume

    ≥ 0.0001 cm³/g

    Degassing Ports

    4 in-situ

    Absorbates

    N₂, Ar, Kr, H₂, O₂, CO₂, CO, NH₃, CH₄, etc.

    Cold Trap

    1

    Volume and Weight

    38.5 in (980 mm) × 25.0 in (630 mm) × 38.5 in (976 mm), 176–199 lbs (≈90 kg)

    Power Requirements

    110 or 200–240 VAC, 50/60 Hz, max power 300 W

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AMI-Sync Series

The AMI-Sync Series is a fully automated gas adsorption analyzer designed for rapid BET surface area, pore size, and porosity characterization of porous and non-porous materials.

AMI
AMI-Sync Series

Gas Adsorption Analyser

  • Multi-port gas adsorption analyser for simultaneous BET and porosity measurements.
  • Complete up to 4 BET surface area measurements in approximately 20–30 minutes under optimized conditions.
  • BET repeatability of ≤ ±1.0% supports accurate, reproducible surface area and pore size analysis.

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The AMI-Sync Series is a fully automated gas adsorption analyzer designed for rapid BET surface area, pore size, and porosity characterization of porous and non-porous materials.

The AMI-Sync Series is a fully automated gas adsorption analyser designed for rapid BET surface area, pore size, and porosity characterisation of porous and non-porous materials. Built for high-throughput laboratory environments, the AMI-Sync supports catalysts, zeolites, MOFs, advanced battery materials, and other materials requiring accurate gas physisorption analysis.

Available in flexible 1-, 2-, or 4-station configurations, the AMI-Sync Series features a common P₀ measuring transducer and supports simultaneous saturation vapor pressure measurements. Each unit is built for high-throughput performance, with options for a dedicated pressure transducer per station to maximize speed, or a shared sensor setup for cost efficiency. A single large-volume dewar supports multiple stations simultaneously, offering an ideal solution for space-conscious laboratories with demanding workloads.

  • Key Features

    Customizable Configuration for Throughput Analysis Needs

    The AMI-Sync series offers a scalable solution with up to four high-resolution measurement stations for precise pore size and surface area analysis. For increased throughput, additional instruments can be linked via LAN, expanding to 12 analysis ports with centralized and remote-control capabilities.

    Extended Analysis Duration

    AMI-Sync analyzers are equipped with large 3-liter Dewar flasks that allow over 90 hours of continuous analysis. The system supports live refilling during experiments, ensuring uninterrupted data collection during long runs and complex isotherm acquisitions.

    High Sensitivity & Reproducibility

    The AMI-Sync Series delivers precise and reliable surface area and porosity data, with a BET detection limit as low as 0.1 m² absolute and 0.01 m²/g specific. It offers outstanding reproducibility—within 1% on standard reference materials like BAM P115—ensuring confidence in repeated analyses.

    Precision-Engineered Hardware

    Built with stainless steel and vacuum-brazed manifolds, the system features ultra-durable bellows valves rated for over 5 million cycles. Temperature control maintains ±0.05 °C stability, while 32-bit pressure sensors provide high-resolution, accurate data capture.

    Cryo TuneTM (Optional Feature)

    Unlock advanced temperature control with Cryo TuneTM, an optional low-temperature cold bath system designed for precision adsorption studies. Fully integrated with Sync software, Cryo TuneTM allows users to effortlessly conduct adsorption isotherm measurements across a range of temperatures.

    Optimized Manifold Contamination Control

    A two-step filtration system protects the manifold from particulates reducing contamination risks and extending instrument life. Combined with stainless steel construction and high-cycle bellows valves, the system ensures clean, reliable operation even in high-throughput environments.

    Compact & Lab-Ready

    All models share a compact footprint of 51 ×53 × 93 cm, making them ideal for space-conscious labs. Despite their compact size, Sync analyzers are fully equipped for both research-grade and industrial applications, offering power, durability, and precision in one system.

  • Software

    Sync Series analyzers are driven by a multilingual, user-friendly software suite that supports:

    • Control of up to 8 instruments from a single PC
    • Built-in method libraries
     for fast setup and repeatability
    • Customizable analysis profiles with real-time system feedback
    • Automated leak detection and guided maintenance routines
    • Visual instrument status interface for monitoring analysis in progress

    Additional capabilities include void volume correction, supercritical P0 handling, temperature control with CryoTune, and compatibility with up to 6 gases per station.

    Data Analysis Capabilities:

    Isothermal absorption and desorption curve
    BET specific surface area (single and multiple point)
    Langmuir surface area
    Statistical thickness surface area. (STSA)

    HK pore size analysis
    SF pore size analysis
    NLDFT pore size distribution
    Total pore volume
    t-plot analysis

  • Specifications

    Specific Model

    110 | 210 | 220 | 420 | 440

    Analysis Ports

    1 | 2 | 2 | 4 | 4

    p0 Transducer

    1 | 1 | 1 | 1 | 1

    Analysis Pressure Transducer

    1 | 1 | 2 | 2 | 4

    Pressure Transducer

    1000 torr

    Pressure Transducer Accuracy and Resolution

    Accuracy: 0.05% F.S., Resolution: 0.0005% F.S

    Specific Surface Area

    ≥ 0.01 m2/g, test repeatability: RSD ≤ ±1.0%

    Pore Size Range

    .35*-500 nm, test repeatability: ≤ ±0.02 nm (*Achieved with CO2)

    Pore Volume

    ≥ 0.0001 cm³/g

    Pump

    1 mechanical pump (ultimate vacuum 10-1 Pa; minimal 7.5 x 10-4 torr)

    P/P0 Range

    10-4 – 0.998

    Absorbates

    N₂, CO₂, Ar, Kr, H₂, O₂, CO, NH₃, CH₄

    Dimensions

    51 × 53 × 93 cm (16.1 × 20.8 × 36.6 inches) – all same size

    Weight

    45 kg | 99 lbs (maximum depending on configuration)

    Power Requirements

    100-240 VAC, 50/60 Hz, maximum power 300 W

  • Applications

    Silver Powder

    Solar Cells

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